Instrumentation

NMR Spectrometer (Bruker Avance III HD 400 MHz), acquired 2016 

  • BCU I Variable Temperature Controller 
  • BBFO Z-Gradient probe for 31P to 15N plus 19F nuclei 
  • SampleXpress 60 position autosampler 

UV-visible absorbance spectrometers

  • Varian Cary 300 Bio, acquired 1999-2004 
  • Ocean Optics USB2000 miniature fiber optic spectrometers 
  • NanoDrop Lite Plus, acquired 2023
  • Cary 3500 with multicell Peltier temperature controller, acquired 2023

IR Spectrometers and microscope

  • Nicolet iS10 with iTX Diamond ATR, acquired 2017
  • Midac M Series, acquired 2000

Polarimeter Jasco P-2000

Atomic absorption spectrometer (Varian SpectrAA 220FS and 220Z), acquired 2003 

  • Flame and graphite furnace atomization 

Fluorescence spectrometer with peltier multicell holder (Varian Cary Eclipse), acquired 2007 

Electrochemical potentiostat/galvanostat (Bioanalytical Systems EC Epsilon), acquired 2005 

Gas chromatography and mass spectrometry 

  • Agilent 5977/8860 with 96 sample autoinjector, acquired 2020 
  • Hewlett Packard 6890/5973 with FID, acquired 1999 

High performance liquid chromatography and mass spectrometry 

  • Waters Alliance e2690 with qDa mass detector and UV-visible dual-wavelength absorbance detector, acquired 2021 
  • Waters Alliance e2690 with UV-visible dual-wavelength absorbance detector and 3D fluorescence detector, acquired 2016 
  • Waters Alliance 515 with UV-visible dual-wavelength absorbance detector, acquired 2001 
  • Water Alliance 2690 with Thermo Finnigan LXQ linear ion trap mass spectrometer, acquired 2004 and 2009 

Preparative Scale Liquid Chromatography 

  • Medium pressure liquid chromatograph/UV-visible absorbance detector and fraction collector (Bio-rad BioLogic DuoFlow/QuadTec and BioFrac), acquired 2009 
  • CombiFlash NextGen 300+ Flash Chromatograph, acquired 2020 

Capillary electrophoresis with laser-induced fluorescence (ABI Prism 310 Genetic Analyzer), acquired 2009 

Glovebox Vacuum Atmospheres Genesis, acquired 2016 

Solvent Purification System Vacuum Atmospheres, acquired 2016 

Formlabs F1 3D-Printer 

Computational Chemistry with Gaussian 16 and WebMO running on Jigwé HPC, acquired 2020

Pulsed Nd:YAG laser (Quanta-Ray LAB-190), acquired 2003